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Calix[2]triazole[2]arenes; A Class of Hybrid Heterocalixarenes
- Issue Date
- 7월-2013
- Publisher
- WILEY-V C H VERLAG GMBH
- Keywords
- Supramolecular chemistry; Calixarenes; Click chemistry; Conformation analysis; Structure elucidation
- Citation
- EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, v.2013, no.21, pp.4614 - 4623
- Indexed
- SCIE
SCOPUS
- Journal Title
- EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
- Volume
- 2013
- Number
- 21
- Start Page
- 4614
- End Page
- 4623
- ISSN
- 1434-193X
- Abstract
- A series of calix[2]triazole[2]arenes, which are members of the heterocalixarene family, were generated by copper(I)-catalyzed Huisgen reaction in a one-pot synthesis. Their various conformational structures and physical properties were characterized by a computational, NMR spectroscopic, and X-ray structural investigation. Among six conformations, the 1,2-alternate conformation was found to be the most stable due to two intramolecular hydrogen bonds between the phenolic hydroxyl group and the triazole nitrogen atom.
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