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Synthesis, Luminescence and Optical Properties of a CaMoO4 Nano-Powder Prepared by Using the Precipitation Method

Authors
Karki, SujitaAryal, PabitraHa, DaehoonKim, Hong JooPark, Hyang KyuPandey, Indra Raj
Issue Date
10월-2019
Publisher
KOREAN PHYSICAL SOC
Keywords
Nano-powder; Precipitation method; X-ray diffraction; Transmittance electron microscopy; Fluorescence decay time
Citation
JOURNAL OF THE KOREAN PHYSICAL SOCIETY, v.75, no.7, pp.534 - 540
Indexed
SCIE
SCOPUS
KCI
Journal Title
JOURNAL OF THE KOREAN PHYSICAL SOCIETY
Volume
75
Number
7
Start Page
534
End Page
540
URI
https://scholar.korea.ac.kr/handle/2021.sw.korea/62613
DOI
10.3938/jkps.75.534
ISSN
0374-4884
Abstract
Nano powders of CaMoO4 were synthesized by using the precipitation method, and the obtained powders were dried inside a vacuum oven at 120 degrees C. The phases of powders were analyzed by using X-ray diffraction (XRD), which revealed that CaMoO4 was free from any extra phases. The surface morphologies of the powders were studied by using transmission electron microscopy (TEM), and the average particle sizes were quite small, being in the range of 7 nm. The optical properties were characterized by using ultraviolet-visible (UV-vis) absorption spectroscopy and the optical energy band gap was found to be 5.51 eV. The fluorescence decay time and the luminescence spectrum of the sample were measured under the excitation by Laser (266 nm), X-ray and proton sources. The obtained results were compared with the CaMoO4 bulk crystal and sintered powder obtained from the solid state reaction.
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