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X-ray diffraction and VT-NMR studies of (E)-3-(piperidinyl)-1-(2 '-hydroxyphenyl)-prop-2-en-1-one

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dc.contributor.authorChoi, Seunghyun-
dc.contributor.authorKim, YunHye-
dc.contributor.authorPark, Bernie Byeonghoon-
dc.contributor.authorPark, Suzie-
dc.contributor.authorPark, Jonghyun-
dc.contributor.authorOk, Kiwon-
dc.contributor.authorKoo, JaeHyung-
dc.contributor.authorJung, Yong Woo-
dc.contributor.authorJeon, Young Ho-
dc.contributor.authorLee, Eun Hee-
dc.contributor.authorLee, Ken S.-
dc.contributor.authorByun, Youngjoo-
dc.date.accessioned2021-09-05T03:05:08Z-
dc.date.available2021-09-05T03:05:08Z-
dc.date.created2021-06-15-
dc.date.issued2014-11-05-
dc.identifier.issn0022-2860-
dc.identifier.urihttps://scholar.korea.ac.kr/handle/2021.sw.korea/96795-
dc.description.abstractA series of 1-aryl-3-(cyclicamino)-prop-2-en-1-one analogs was synthesized from commercial acetophenones in 2 or 3 steps. Compound 6, (E)-3-(piperidinyl)-1-(2'-hydroxyphenyl)-prop-2-en-1-one, exhibited the unique shape and intensity of the C-sp2-N-CH2 peaks in the H-1 and C-13 NMR spectra. Variable temperature (VT) nuclear magnetic resonance (NMR) and X-ray diffraction (XRD) studies of 6 revealed that the piperidine ring has a lower energy barrier to rotation than the 5-membered pyrrolidine 9 due to the less effective pi electron delocalization along the C-sp2-N bond. (C) 2014 Elsevier B.V. All rights reserved.-
dc.languageEnglish-
dc.language.isoen-
dc.publisherELSEVIER-
dc.subjectENAMINONES-
dc.subjectBENZOYLACETONE-
dc.subjectCONDENSATION-
dc.subjectTAUTOMERISM-
dc.subjectDERIVATIVES-
dc.subjectPRODUCTS-
dc.titleX-ray diffraction and VT-NMR studies of (E)-3-(piperidinyl)-1-(2 '-hydroxyphenyl)-prop-2-en-1-one-
dc.typeArticle-
dc.contributor.affiliatedAuthorJung, Yong Woo-
dc.contributor.affiliatedAuthorJeon, Young Ho-
dc.contributor.affiliatedAuthorLee, Eun Hee-
dc.contributor.affiliatedAuthorByun, Youngjoo-
dc.identifier.doi10.1016/j.molstruc.2014.08.016-
dc.identifier.scopusid2-s2.0-84907291626-
dc.identifier.wosid000343613400078-
dc.identifier.bibliographicCitationJOURNAL OF MOLECULAR STRUCTURE, v.1076, pp.600 - 605-
dc.relation.isPartOfJOURNAL OF MOLECULAR STRUCTURE-
dc.citation.titleJOURNAL OF MOLECULAR STRUCTURE-
dc.citation.volume1076-
dc.citation.startPage600-
dc.citation.endPage605-
dc.type.rimsART-
dc.type.docTypeArticle-
dc.description.journalClass1-
dc.description.journalRegisteredClassscie-
dc.description.journalRegisteredClassscopus-
dc.relation.journalResearchAreaChemistry-
dc.relation.journalWebOfScienceCategoryChemistry, Physical-
dc.subject.keywordPlusENAMINONES-
dc.subject.keywordPlusBENZOYLACETONE-
dc.subject.keywordPlusCONDENSATION-
dc.subject.keywordPlusTAUTOMERISM-
dc.subject.keywordPlusDERIVATIVES-
dc.subject.keywordPlusPRODUCTS-
dc.subject.keywordAuthorEnaminones-
dc.subject.keywordAuthorX-ray diffraction-
dc.subject.keywordAuthorVT-NMR-
dc.subject.keywordAuthorFlexible rotation-
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