Calix[2]triazole[2]arenes; A Class of Hybrid Heterocalixarenes

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초록

A series of calix[2]triazole[2]arenes, which are members of the heterocalixarene family, were generated by copper(I)-catalyzed Huisgen reaction in a one-pot synthesis. Their various conformational structures and physical properties were characterized by a computational, NMR spectroscopic, and X-ray structural investigation. Among six conformations, the 1,2-alternate conformation was found to be the most stable due to two intramolecular hydrogen bonds between the phenolic hydroxyl group and the triazole nitrogen atom.

키워드

Supramolecular chemistryCalixarenesClick chemistryConformation analysisStructure elucidationSELECTIVE RECOGNITIONFLUORESCENCE SENSORTRIAZOLECONJUGATEMACROCYCLEZN2+CYCLOADDITIONSPYROPHOSPHATECONSTRUCTIONSUBSTITUENTS
제목
Calix[2]triazole[2]arenes; A Class of Hybrid Heterocalixarenes
저자
Cho, JiheeLee, SeokwooHwang, SoonhoKim, Sang HoonKim, Jong SeungKim, Sanghee
DOI
10.1002/ejoc.201300401
발행일
2013-07
유형
Article
저널명
European Journal of Organic Chemistry
2013
21
페이지
4614 ~ 4623