Stereoselective Synthesis of Anti-Hepatitis B Drug, Entecavir, through Regio- and Stereoselective Epoxide Cleavage

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초록

A stereoselective synthesis of entecavir, an anti-hepatitis B (HBV) drug, was accomplished by a regioselective isopropylidene cleavage, stereoselective Sharpless epoxidation, and Ti-III-mediated regio- and stereoselective epoxide cleavage as key steps.

키워드

carbocyclic nucleosideentecavirhepatitis BStereoselective synthesistitaniumVERSATILE INTERMEDIATE2,3-EPOXY ALCOHOLSBMS-200475MECHANISMKETONESPOTENTVIRUS INFECTIONASYMMETRIC EPOXIDATION
제목
Stereoselective Synthesis of Anti-Hepatitis B Drug, Entecavir, through Regio- and Stereoselective Epoxide Cleavage
저자
Hyun, Young EumKim, Hong-RaeChoi, YongseokJeong, Lak Shin
DOI
10.1002/ajoc.201700032
발행일
2017-09
유형
Article
저널명
Asian Journal of Organic Chemistry
6
9
페이지
1213 ~ 1218