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Tetraglyme-mediated synthesis of Pd nanoparticles for dehydrogenation of ammonia borane
- Authors
- Kim, Sung-Kwan; Kim, Tae-Jin; Kim, Tae-Young; Lee, Gaehang; Park, Joon T.; Nam, Suk Woo; Kang, Sang Ook
- Issue Date
- 2012
- Publisher
- ROYAL SOC CHEMISTRY
- Citation
- CHEMICAL COMMUNICATIONS, v.48, no.14, pp.2021 - 2023
- Indexed
- SCIE
SCOPUS
- Journal Title
- CHEMICAL COMMUNICATIONS
- Volume
- 48
- Number
- 14
- Start Page
- 2021
- End Page
- 2023
- ISSN
- 1359-7345
- Abstract
- Palladium nanoparticles (PdNPs) were conveniently prepared in tetraglyme (TG) solution using a variety of palladium precursors. At 140 degrees C, TG promoted Pd-3(OAc)(6) to produce irregular shaped PdNPs with an average size of 4 nm. When these PdNPs were re-dispersed in TG and used for the dehydrogenation of ammonia borane (AB) at 85 degrees C, remarkably enhanced catalytic performance was achieved to release 2.3 equiv. of H-2 in 1 h.
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