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Expedient synthesis of 4-O-methylhonokiol via Suzuki-Miyaura cross-coupling
- Authors
- Kwak, Jae-Hwan; Cho, Young Ae; Jang, Jae-Yong; Seo, Seung-Yong; Lee, Heesoon; Hong, Jin Tae; Han, Sang-Bae; Lee, Kiho; Kwak, Young-Shin; Jung, Jae-Kyung
- Issue Date
- 2-12월-2011
- Publisher
- PERGAMON-ELSEVIER SCIENCE LTD
- Keywords
- Neolignan; 4-O-Methylhonokiol; Suzuki-Miyaura cross-coupling; Potassium aryltrifluoroborate
- Citation
- TETRAHEDRON, v.67, no.48, pp.9401 - 9404
- Indexed
- SCIE
SCOPUS
- Journal Title
- TETRAHEDRON
- Volume
- 67
- Number
- 48
- Start Page
- 9401
- End Page
- 9404
- ISSN
- 0040-4020
- Abstract
- Concise and practical synthesis of 4-O-methylhonokiol was achieved in 34% overall yield. The key features of our synthesis include chemoselective ortho-mono bromination of phenol as well as biaryl formation via Suzuki-Miyaura cross-coupling, in which bromophenol was reacted with potassium aryltrifluoroborate using Pd(OAc)(2) and RuPhos under microwave conditions. (C) 2011 Elsevier Ltd. All rights reserved.
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