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Low Temperature Synthesis of Single Crystalline Iron Hydroxide and Oxide Nanorods in Aqueous Media

Authors
Chaudhari, Nitin K.Fang, BaizengBae, Tae-SungYu, Jong-Sung
Issue Date
5월-2011
Publisher
AMER SCIENTIFIC PUBLISHERS
Keywords
Iron Hydroxide (beta-FeOOH); Magnetic; Caffeine; Iron Oxide
Citation
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, v.11, no.5, pp.4457 - 4462
Indexed
SCIE
SCOPUS
Journal Title
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
Volume
11
Number
5
Start Page
4457
End Page
4462
URI
https://scholar.korea.ac.kr/handle/2021.sw.korea/112513
DOI
10.1166/jnn.2011.3687
ISSN
1533-4880
Abstract
An easy aqueous 'one-pot' synthesis route for the fabrication of single crystalline uniform iron hydroxide (beta-FeOOH) nanorods at low temperature is reported. beta-FeOOH nanorods with diameters of 5-37 nm and lengths up to 45-185 nm were obtained by varying the reaction parameters. Addition of ethanol was found to be crucial to control the aspect ratio. After calcination at 250 degrees C for 2 h the as-obtained beta-FeOOH nanorods was converted to alpha-Fe2O3 nanorods. To the best of our knowledge, beta-FeOOH nanorods having diameter less than 6 nm is reported for the first time.
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