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Efficient Palladium-Catalyzed Coupling of Baylis-Hillman Acetates with an Allylstannane

Authors
Park, JinhyungKwon, Young BumYang, KyungmoRhee, HakjuneYoon, Cheol Min
Issue Date
Feb-2010
Publisher
GEORG THIEME VERLAG KG
Keywords
Baylis-Hillman acetates; allyltributylstannane; bis-pi-allylpalladium; 1,5-diene; allylation
Citation
SYNTHESIS-STUTTGART, no.4, pp.661 - 665
Indexed
SCIE
SCOPUS
Journal Title
SYNTHESIS-STUTTGART
Number
4
Start Page
661
End Page
665
URI
https://scholar.korea.ac.kr/handle/2021.sw.korea/117130
DOI
10.1055/s-0029-1218612
ISSN
0039-7881
Abstract
Acetates of Baylis-Hillman adducts derived from ethyl acrylate, methyl vinyl ketone, and acrylonitrile were coupled with allyltributylstannane using Pd(PPh3)(4) or Pd(dba)(2) as the catalyst at room temperature to afford the corresponding trisubstituted alka-1,5-dienes in good to high yields.
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