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Metal nanoparticle synthesis using supercritical alcohol

Authors
Kim, JaehoonKim, DaewooVeriansyah, BambangKang, Jeong WonKim, Jae-Duck
Issue Date
31-8월-2009
Publisher
ELSEVIER SCIENCE BV
Keywords
Nanomaterials; Metal nanoparticles; Supercritical fluids
Citation
MATERIALS LETTERS, v.63, no.21, pp.1880 - 1882
Indexed
SCIE
SCOPUS
Journal Title
MATERIALS LETTERS
Volume
63
Number
21
Start Page
1880
End Page
1882
URI
https://scholar.korea.ac.kr/handle/2021.sw.korea/119471
DOI
10.1016/j.matlet.2009.05.066
ISSN
0167-577X
Abstract
Metal nanoparticles with uniform size distribution were synthesized in a low carbon number of supercritical alcohol without using reducing agents or surfactants. Nanoparticles of copper (Cu). nickel (Ni). and silver (Ag) were synthesized in supercritical methanol or supercritical ethanol at 300 bar, 400 degrees C and reaction time of 5 min. The supercritical alcohol acted both as reaction medium and as a reducing agent. The synthesized particles were spherical in shape. The average diameter of Cu, Ni, and Ag particles was 420 +/- 119 nm, 50 +/- 10 nm, and 390 +/- 114 nm, respectively. Crown Copyright (C) 2009 Published by Elsevier B.V. All rights reserved.
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