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A proline-based macrocyclic amide with S-4 symmetry
- Authors
- Ahn, Hee Choon; Yun, Sun-mi; Choi, Kihang
- Issue Date
- 5-1월-2008
- Publisher
- CHEMICAL SOC JAPAN
- Citation
- CHEMISTRY LETTERS, v.37, no.1, pp.10 - 11
- Indexed
- SCIE
SCOPUS
- Journal Title
- CHEMISTRY LETTERS
- Volume
- 37
- Number
- 1
- Start Page
- 10
- End Page
- 11
- ISSN
- 0366-7022
- Abstract
- A new square-shaped macrocyclic amide was prepared from N-(4-amino-2-nitrophenyl)proline (ANPP). The two enantiomers of ANPP were connected in an alternating sequence and then cyclized to the corresponding macrocyclic tetramer with S-4 symmetry. In this design, there is a central cavity approximately 7 angstrom in diameter and rigid aromatic rings and intramolecular hydrogen bonding help to reduce the conformational flexibility of the molecule.
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