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Generation and reaction of cyano-substituted aryllithium compounds using microreactors

Authors
김희진
Issue Date
Mar-2010
Publisher
ROYAL SOC CHEMISTRY
Citation
ORGANIC & BIOMOLECULAR CHEMISTRY, v.8, no.5, pp.1212 - 1217
Indexed
SCIE
SCOPUS
Journal Title
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume
8
Number
5
Start Page
1212
End Page
1217
URI
https://scholar.korea.ac.kr/handle/2021.sw.korea/140054
DOI
10.1039/b919325c
ISSN
1477-0520
Abstract
We developed a microflow method for the generation and reactions of aryllithiums bearing a cyano group, including o-lithiobenzonitrile, m-lithiobenzonitrile and p-lithiobenzonitrile. The method was effective at much higher temperatures than are required for conventional macrobatch reactions, by virtue of rapid mixing, short residence time, and efficient temperature control. In addition, reactions of o-lithiobenzonitrile with carbonyl compounds followed by trapping of the resulting lithium alkoxides with electrophiles were achieved in an integrated microflow system.
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