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Photocurable ceramic slurry using solid camphor as novel diluent for conventional digital light processing (DLP) process

Authors
Lee, Yun-HeeLee, Jung-BinMaeng, Woo-YoulKoh, Young-HagKim, Hyoun-Ee
Issue Date
11월-2019
Publisher
ELSEVIER SCI LTD
Keywords
Additive manufacturing; Porous ceramics; Photopolymerization; Camphor; Diluent
Citation
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, v.39, no.14, pp.4358 - 4365
Indexed
SCIE
SCOPUS
Journal Title
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
Volume
39
Number
14
Start Page
4358
End Page
4365
URI
https://scholar.korea.ac.kr/handle/2021.sw.korea/62105
DOI
10.1016/j.jeurceramsoc.2019.05.069
ISSN
0955-2219
Abstract
This study presents the utility of solid camphor as a novel type of diluent for the preparation of photocurable ceramic slurries with sufficiently low viscosity at high solid loading (48 vol%), which can be applicable for the conventional digital light processing (DLP) process. The camphor addition remarkably decreased the viscosity of calcium phosphate (CaP) ceramic slurries without affecting their photopolymerization behavior. This approach could effectively mitigate the clogging of pores with residual slurries, and thus the porous structure of porous CaP scaffolds with 3D channels could be tightly controlled. Furthermore, the high densification of CaP frameworks after sintering at 1250 degrees C for 3 h could be achieved owing to the use of the high solid loading in the CaP slurry. The porous CaP scaffolds produced displayed high compressive strength ((similar to)23.8 MPa) and modulus ((similar to)276 MPa) at a high porosity of (similar to)50.6 vol%.
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