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In situ generation of hydroperoxide by oxidation of benzhydrols to benzophenones using sodium hydride under oxygen atmosphere: use for the oxidative cleavage of cyclic 1,2-diketones to dicarboxylic acids
- Authors
- Kang, Sunhae; Lee, Soyoung; Jeon, Minju; Kim, Sun Min; Kim, Young Sug; Han, Hogyu; Yang, Jung Woon
- Issue Date
- 30-1월-2013
- Publisher
- PERGAMON-ELSEVIER SCIENCE LTD
- Keywords
- Oxidative cleavage; Cyclic 1,2-diketone; Dicarboxylic acid; Sodium hydride; Benzhydrol
- Citation
- TETRAHEDRON LETTERS, v.54, no.5, pp.373 - 376
- Indexed
- SCIE
SCOPUS
- Journal Title
- TETRAHEDRON LETTERS
- Volume
- 54
- Number
- 5
- Start Page
- 373
- End Page
- 376
- ISSN
- 0040-4039
- Abstract
- A facile oxidative cleavage of cyclic 1,2-diketones 1 to dicarboxylic acids 3 with hydroperoxide generated in situ has been developed. In situ generation of hydroperoxide was effected by the oxidation of 4,4'-dichlorobenzhydrol 2f to 4,4'-dichlorobenzophenone 41 using sodium hydride under oxygen atmosphere. (C) 2012 Elsevier Ltd. All rights reserved.
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